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Spectroelectrochemical set-up

Spectroelectrochemistry (SEC) is aimed at the investigation of electrochemical reaction mechanism and the interface structure between electrolyte solution and electrode. Remarkable progress in this field and related technology enables SEC to be applied in wide areas. Nowadays, the relation between absorbance and potential for reversible or quasi-reversible system is theoretically elucidated, on which basis the analysis of electrochemical characteristics becomes possible for the system otherwise difficult with only the result of voltammogram.

Here, we will introduce two systems set-up (flow system and batch), for spectroelectrochemical measurement.

  • Flow system
  • Batch system
  • Related product
Schematic diagram for Spectroelectrochemical measurement in flow system. 1. SEC2000-UV/VIS
    Spectrometer
2. SEC2000
    Light Source
3. SEC-2F
    Spectroelectrochemical
    flow cell
4. Reference electrode
5. UV/VIS
    Collimating Lens
6. Optical fiber
7. Electrochemical
    analyzer
8. PC


1 SEC2000 -UV/VIS Spectrometer is a multichannel spectrometer, specially designed for Spectroelectrochemical measurement.
2 SEC2000 - Light source.
3 SEC-2F Spectroelectrochemical flow cell.
4 Reference electrode, it is sold separately.
There is two types: for aqueous solution (RE-3V Reference electrode Screw type (Ag/AgCl)) and for non aqueous solution (RE-7V Non Aqueous reference electrode (Ag/Ag+) Screw type).
5 74-UV UV/VIS Collimating Lens for the conection between probe type of optical fiber and light source.
6 SMA 905 Connectors teminate optical fiber.
7 Electrochemical analyzer
8 The minimum recommended PC configuration is windowsOS 8.1, CPU Intel Core i3.



For general application without SEC2000 Spectrometer system

Schematic diagram for Spectroelectrochemical measurement in batch system. 1. SEC2000 Spectrometer
2. SEC-C SEC-C Thin
    Layer Quartz Glass
    Spectroelectrochemical
    cell Kit
3. Reference electrode
4. Electrochemical
    analyzer
5. PC







1 SEC2000 - UV/VIS Spectrometer is a multichannel spectrometer, specially designed for Spectroelectrochemical measurement.
2 SEC-C SEC-C Thin Layer Quartz Glass Spectroelectrochemical cell Kit
Components of the SEC-C:
- SEC-C Pt or Au Gauze working electrode
- SEC-C Pt counter electrode
- SEC-C Thin Layer Quartz Glass cell
- SEC-C Teflon Cap
- Purge tube (ETFE)
3 Reference electrode, it is sold separately.
There is two types: for aqueous solution (RE-1B Silver-Silver chloride reference electrode) and for non aqueous solution (RE-7 Non Aqueous reference electrode)
4 Electrochemical analyzer
5 The minimum recommended PC configuration is Pentium 120 MHz, RAM 16 MB with more than 256 color VGA card. 486 PC is also compatible while the data process speed of CPU could be caused. SEC2000 software is compatible with Windows 95, 98, 2000 and XP.





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