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RRDE-3A Rotating Ring Disk Electrode Apparatus Ver1.2 (cat#012623)

Rotating Ring Disk Electrode Rotator (RRDE-3) apparatus
 


RRDE-3A is a constant rotation system for use in hydrodynamic modulation rotating ring disk electrochemistry. A 7 mm diameter electrode with short stainless steel shaft provides for a miniature and concentric circle electrode system that is capable for highly accurate rotation and modulation even at radial modulation rates or wave forms.

RRDE-3A is precisely controlled by PPL (Phase Locked Loop) signal. Electrodes are small and rapidly interchangeable. The unit also provides an adjustable valve system for inert gas purging inside the cell vial.

RRDE-3A is able to be operated as a stand-alone unit and directly controlled by CH Instrumetns, Inc., Bioanalytical Systems, Inc. electrochemical analyzers, model2325 or other instruments. When the analysis starts, a built-in gas control allows purging the sample.

Besides, the access to glass cell is easy for rinsing, cleaning, and replacing the electrodes. It is easy to remove and replace the cell vial.

Troubleshooting

Technical Note
Hydrodynamic Voltammetry


Other potentiostats
Connections

  • Operating
  • Specifications & Features
  • RRDE-3A content
  • Working Electrode
  • Movies

Specifications

Rotational range 100 to 8,000 rpm
Rotation stability Error, < 2% at < 2,000 rpm
        < 1% at > 2,000 rpm
Ring/Disk insulation resistance > 10 M ohm
Electrode to lead pin contact resistance 5 ohm
Rotator shaft Stainless steel
Motor 12 V, ironless core, low inertial DC servo
Power 100-240 VAC, 50/60 Hz
Remote control One volt corresponds to 1,000 rpm
Motor ON/OFF TTL or relay input to back panel connection
Purge TTL or relay input to back panel connection
Size 190 x (Base: 230, Body: 120) x 400 mm
Weight 6 kg
Operating temperature 10 to 50°C
Relative humidity ≤ 80%



Features

  • Operable as RDE and RRDE
  • Remote and manual controlled rotation and gas purge
  • Gas line connector is available
  • Cell lead connects to all potentiostats
  • Open architecture for easy access to cell
  • Compact design & easy operation
  • Shaft is completely insulated for the motor by coupling unit to reduce motor noise
  • In the shaft assembly, the inner and outer tube is completely insulated by Teflon spacer to reduce noise
Cat# Description
012623 RRDE-3A Rotating Ring Disk Electrode Apparatus Ver.1.2
Contents
012632 Sample vial (100 mL)
013271 RRDE-3A Teflon cap V.2
012064 Spin coating adaptor
012065 Male connector for gas purge (PP)
013392 TYGON tubing, OD1/4 x ID1/8
012642 RRDE-3A Sillicon sheet 100x180 mm
012976 O-ring for RRDE-3A shaft assembly, 3 pcs
012975 O-ring for RRDE-3A Bearing assembly, 3 pcs
Power supply cable
Instruction manual
Optional items
012167 RE-1B Reference electrode (Ag/AgCl)
012171 RE-7 Non Aqueous reference electrode (Ag/Ag+)
013373 RHEK Reversible hydrogen electrode kit
012961 Platinum counter electrode 23 cm
012962 Gold counter electrode 23 cm
012963 Nickel counter electrode 23 cm
013580 Sample vial for alkaline solution (100 mL) (10 pcs)
013581 Sample vial for alkaline solution (200 mL) (8 pcs)
013582 RRDE-3A Teflon cap (for 200 mL)
013343 O-ring for RRDE-3A Teflon cap V.2
012829 O-ring for RRDE-3A Shaft assembly (10 pcs)
012641 O-ring for RRDE-3A Bearing assembly (10 pcs)
Option
For RRDE electrode
RRDE electrode
Click here for detail
Platinum ring disk working electrode
Platinum ring-glassy carbon disk working electrode
For RDE electrode
RDE electrode
Click here for detail
Glassy carbon disk electrode
Platinum working disk electrode
Gold working disk electrode
For DRE electrode
DRE electrode
Click here for detail
DRE-PGK Pt ring/GC disk replaceable electrode
DRE-GCK disk replaceable electrode
Electrodes of other materials and diameters will be fabricated on a custom basis.

Movie contents

  • RRDE-3A easy setup
  • RRDE-3A disassembling/assembling for maintenance
  • RRDE-3A motor rotation issue
  • DRE electrode assembly methods Part1: Front Assembly
  • DRE electrode assembly methods Part2: Rear Assembly

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